The use of pulsed Fourier transform 1H n.m.r. spectroscopy has been shown to give detailed information concerning the protonation sites of the catecholamines; in particular, a method for the assignment of the microconstants for the deprotonation of L-dopa and the determination of their values has been rigorously established.
R. F. Jameson, G. Hunter and T. Kiss, J. Chem. Soc., Chem. Commun., 1978, 768 DOI: 10.1039/C39780000768
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