The phenaleno[1,9-cd]dithiolyl radical has been prepared in solution by electrochemical and chemical reduction of phenaleno[1,9-cd]dithiolium hexafluorophosphate; it has been studied by e.s.r., mass, and electronic spectroscopy, and is monomeric in solution in the temperature range 19 to –95°C.
R. C. Haddon, F. Wudl, M. L. Kaplan, J. H. Marshall and F. B. Bramwell, J. Chem. Soc., Chem. Commun., 1978, 429 DOI: 10.1039/C39780000429
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