Nitroxyl (nitrosyl hydride), HNO, has been generated by the dissociation of 9,10-dihydro-9,10-epoxyimino-9,10-dimethylanthracene at 70 °C and studied by microwave spectroscopy in the range 18–32 GHz.
J. E. T. Corrie, G. W. Kirby, A. E. Laird, L. W. Mackinnon and J. K. Tyler, J. Chem. Soc., Chem. Commun., 1978, 275 DOI: 10.1039/C39780000275
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