Oxyl radicals have been found to be formed from various types of hindered nitro-compounds by photolysis under degassed conditions. This observation is strong evidence which supports the formation of nitrites by photochemical rearrangements of nitro-groups. This report discusses the usefulness of the reaction for the identification of oxyl radicals.
Y. Ioki, J. Chem. Soc., Perkin Trans. 2, 1977, 1240 DOI: 10.1039/P29770001240
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