Methyl 3-O-benzoyl-2,6-dideoxy-4-O-methyl-α-D-ribo-hexopyranoside (10) has been synthesised by an unambiguous route from methyl 4,6-O-benzylidene-2-deoxy-α-D-ribo-hexopyranoside (2). The benzoate (10) differs from benzoylated methyl varioside (obtained by way of methanolysis of the antibiotic variamycin), which is claimed to have the same structure.
J. S. Brimacombe, A. S. Mengech and L. C. N. Tucker, J. Chem. Soc., Perkin Trans. 1, 1977, 643 DOI: 10.1039/P19770000643
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