X-{A} INDOR spectra greatly simplify the analysis of tetrahedral [AX]4 systems. The method is illustrated by the determination of the magnitudes and relative signs of 1J(PF), 3J(PF), 2J(PP), and 4J(FF) in complexes [ML4][M = Ni or Pt; L = F[graphic omitted] or PF(OPh)2].
C. Crocker and R. J. Goodfellow, J. Chem. Soc., Dalton Trans., 1977, 1687 DOI: 10.1039/DT9770001687
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