The determination of fluorine in silicate materials with a fluoride ion-selective electrode following fusion with lithium metaborate is described. The method is rapid, and the values obtained compare well with accepted values for standard rock and mineral samples. Samples containing up to 2.7% of fluorine have been analysed by this method.
J. B. Bodkin, Analyst, 1977, 102, 409 DOI: 10.1039/AN9770200409
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