SCHEDULED MAINTENANCE
Peroxodisulphuryl difluoride, (FSO3)2, generated by constant-current electrolysis of fluorosulphuric acid–potassium fluorosulphate (1.0M), reacts rapidly and smoothly with a series of carboxylic acids (C3–C10) in fluorosulphuric acid at 273 K. Oxidation occurs at a site remote from the carboxy-group and, after work-up, lactones can be isolated in high yields.
C. J. Myall, D. Pletcher and C. Z. Smith, J. Chem. Soc., Perkin Trans. 1, 1976, 2035 DOI: 10.1039/P19760002035
To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.
If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.
If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.
Read more about how to correctly acknowledge RSC content.
Please wait while we load your content...