The application of the Koenigs–Knorr and Lemieux–Nagabhushan reactions to the synthesis of a variety of novel 4-O-pentofuranosyl and 4-O-pentopyranosyl derivatives of garamine is described. The solution conformations of these novel pentosyl aminocyclitols have been assigned on the basis of 13C n.m.r. data.
A. K. Mallams, S. S. Saluja, D. F. Crowe, G. Detre, M. Tanabe and D. M. Yasuda, J. Chem. Soc., Perkin Trans. 1, 1976, 1135 DOI: 10.1039/P19760001135
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