The title compound (IIe) crystallises in the orthorhombic space group Pbca, with a= 26.70(2). b= 9.858(8), c= 11.38(1)Å, and Z= 8. The structure has been solved by direct statistical methods and refined by least-squares to R 9.2% for 1 429 observed reflections. Each dioxaphosphorinane ring has a chair conformation with the phosphoryl oxygen in the equatorial position.
D. S. Cook and R. F. M. White, J. Chem. Soc., Dalton Trans., 1976, 2212 DOI: 10.1039/DT9760002212
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