Toluene-p-sulphonylnitrene (II) can be generated from NN-dichlorotoluene-p-sulphonamide (I) by electrolysis, as shown by the formation of 2-(p-tolylsulphonylamino)-1,4-dioxan (III) in the electroreduction of (I) in the presence of dioxan.
T. Fuchigami, T. Nonaka and K. Iwata, J. Chem. Soc., Chem. Commun., 1976, 951 DOI: 10.1039/C39760000951
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