Single-crystal studies on NbS2(C5H5N)0.5 and NbS2(C5D5N)0.5 by neutron diffraction established a position of the pyridine ring with the aromatic plane perpendicular to the metal sulphide layers and the nitrogen atom located midway between adjoining layered units.
C. Riekel, D. Hohlwein and R. Schöllhorn, J. Chem. Soc., Chem. Commun., 1976, 863 DOI: 10.1039/C39760000863
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