Solid-state thermolysis at 90°C or photolysis at ambient temperature of the molecular complex of deoxycholic acid with di-t-butyl diperoxycarbonate leads to a one-step regiospecific and stereospecific hydroxylation at position 5 of the acid.
N. Friedman, M. Lahav, L. Leiserowitz, R. Popovitz-Biro, C. Tang and Z. (V. I.) Zaretzkii, J. Chem. Soc., Chem. Commun., 1975, 864 DOI: 10.1039/C39750000864
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