A nuclear magnetic double resonance method for determining the sign and magnitude of J(XX) in [AnX]2Mp spin systems by observation of the M resonance only is described, and is applied to some representative diphosphorus compounds.
I. J. Colquhoun, J. D. Kennedy, W. McFarlane and R. J. Puddephatt, J. Chem. Soc., Chem. Commun., 1975, 638 DOI: 10.1039/C39750000638
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