A new, general, stepwise porphyrin synthesis in which tripyrrenes (2) and 1′,8′-dimethyl-a,c-biladienes (9) are crystalline and fully characterised intermediates is exemplified in the first total synthesis of isocoproporphyrin tetramethyl ester (1).
J. A. P. B. de Almeida, G. W. Kenner, K. M. Smith and M. J. Sutton, J. Chem. Soc., Chem. Commun., 1975, 111 DOI: 10.1039/C39750000111
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