The structures of three macrocyclic thioethers with ring sizes varying from 12 to 18 atoms have been detremined by X-ray diffraction and the donor atoms have been found to be nearly coplanar with the sulphur atoms directed out of the ring.
N. K. Dalley, J. S. Smith, S. B. Larson, K. L. Matheson, J. J. Christensen and R. M. Izatt, J. Chem. Soc., Chem. Commun., 1975, 84 DOI: 10.1039/C39750000084
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