(D3)-Trishomocubane (I) can be synthesized easily by aluminum bromide-catalysed isomerization of pentacyclo[5,4,0,0,2,603,10,05,9]undecane (II) or by skeletal rearrangement during aqueous HI iodination of the diol (III), followed by dehalogenation.
S. A. Godleski, P. v. R. Schleyer, E. Ōsawa and G. J. Kent, J. Chem. Soc., Chem. Commun., 1974, 976b DOI: 10.1039/C3974000976B
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