The crystal and molecular structure of the [Co(CN)5]3– anion has been determined; the complex has square-pyramidal geometry with a trans Cbasal–Co–Cbasal angle of 164·7(4)° and Co–Capical and Co–Cbasal bond lengths of 2·01 and 1·89 Å, respectively.
L. D. Brown and K. N. Raymond, J. Chem. Soc., Chem. Commun., 1974, 910b DOI: 10.1039/C3974000910B
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