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It has been established that arugosin C, C25H28O6, an optically active metabolite of A. rugulosus, has the dibenz-[b,e]oxepin structure (IV) and is, therefore, closely related to arugosin A. This structure was established by mass spectrometry and by a comparison of the 1H and 13C n.m.r. spectra with those of arugosin A.
J. A. Ballantine, V. Ferrito, C. H. Hassall and M. L. Jenkins, J. Chem. Soc., Perkin Trans. 1, 1973, 1825 DOI: 10.1039/P19730001825
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