Treatment of hex-2-enopyranosides with chlorosulphonyl isocyanate gives 3-alkoxycarbonylamino-3-deoxyglycals. 1,2-O-Isopropylidene groups in sugars are removed by the reagent and 1,2-carbonates are formed.
R. H. Hall, A. Jordaan and G. J. Lourens, J. Chem. Soc., Perkin Trans. 1, 1973, 38 DOI: 10.1039/P19730000038
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