Quaternary 13C n.m.r. singals may be increased relative to those from hydrogen bearing carbon atoms, whose signals are vastly reduced or eliminated, by the use of very low powers for broad-band decoupling.
I. H. Sadler, J. Chem. Soc., Chem. Commun., 1973, 809 DOI: 10.1039/C39730000809
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