I.r. spectroscopic evidence is presented for the formation of Ni(CO)–3 from the vacuum u.v. photolysis of Ni(CO)4 in low temperature matrices; photolysis of Cr(CO)6 under similar conditions gives bands previously assigned to Cr(CO)–5, and of Fe(CO)5 two new bands probably due to Fe(CO)4–.
J. K. Burdett, J. Chem. Soc., Chem. Commun., 1973, 763 DOI: 10.1039/C39730000763
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