A single-crystal X-ray structure analysis of Prussian Blue, Fe4[Fe(CN)6]3,14H2O, reveals that the space group symmetry of the approximate structure is Oh5-Fm3m with occupancy factors of 0·75 for FeII, C, and N; the more detailed investigation demonstrates deviations from the cubic face-centred symmetry.
H. J. Buser, A. Ludi, W. Petter and D. Schwarzenbach, J. Chem. Soc., Chem. Commun., 1972, 1299 DOI: 10.1039/C39720001299
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