Osmium oxide tetrafluoride OsOF4 has been prepared in good yield by the reduction of OsOF5 on a hot tungsten filament and has been characterized by chemical analysis, molecular beam mass spectroscopy, and X-ray crystallography.
W. E. Falconer, R. D. Burbank, G. R. Jones, W. A. Sunder and M. J. Vasile, J. Chem. Soc., Chem. Commun., 1972, 1080 DOI: 10.1039/C39720001080
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