A novel heteronuclear triple resonance technique is used to obtain 77Se chemical shifts in organophosphorus selenides, and to show that the dipolar form of the phosphorus–selenium link is predominant.
W. McFarlane and D. S. Rycroft, J. Chem. Soc., Chem. Commun., 1972, 902 DOI: 10.1039/C39720000902
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