The variable-temperature 19F n.m.r. spectra of the hexafluoroacetone adducts of a series of 1-substituted phosphetans give data on the relative apicophilicities of different groups which are interpreted in terms of electronegativity and back-bonding factors.
R. K. Oram and S. Trippett, J. Chem. Soc., Chem. Commun., 1972, 554 DOI: 10.1039/C39720000554
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