A single crystal X-ray diffraction study of spectinomycin dihydrobromide pentahydrate has shown that the molecule has a B/Ccis ring juncture and exists as a stable ketone hydrate; the absolute configuration of the molecule was determined by anomalous dispersion.
T. G. Cochran, D. J. Abraham and L. L. Martin, J. Chem. Soc., Chem. Commun., 1972, 494 DOI: 10.1039/C39720000494
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