SCHEDULED MAINTENANCE
Reactions of trisubstituted phosphines with bis(trifluoromethyl) peroxide and bis(trifluoromethyl) disulphide proceed rapidly at –78° to give difluorophosphoranes, one of which (II) exists as a slowly equilibrating mixture at low temperatures.
N. J. De'Ath, D. Z. Denney and D. B. Denney, J. Chem. Soc., Chem. Commun., 1972, 272 DOI: 10.1039/C39720000272
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