A method has been developed for the quantitative determination of bisthiosemicarbazones in which addition of copper(II) chloride to a solution of the organic compound leads to complex formation. The hydrogen ions liberated on complex formation are determined by potentiometric titration. The complex, or the organic ligand itself, can also be determined spectrophotometrically.
M. J. M. Campbell, R. Grzeskowiak, G. G. Jenkinson and I. D. M. Turner, Analyst, 1972, 97, 70 DOI: 10.1039/AN9729700070
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