Capreomycidine (II) and epicapreomycidine (VIII) have been synthesised by hydrogenation and hydrolysis of 2-amino-4-(α-methoxycarbonyl-α-hydroxyimino)methylpyrimidine (VII; R = CO2Me, R1= H). A similar sequence of reactions with the 6-methoxy- or 6-hydroxy-analogues failed to yield viomycidine.
B. W. Bycroft, D. Cameron and A. W. Johnson, J. Chem. Soc. C, 1971, 3040 DOI: 10.1039/J39710003040
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