The n.m.r. spectra of 14 asymmetrically substituted 1,3-dioxans have been examined and their temperature-dependence has provided information on the conformational requirements of the substituents. Thermodynamic parameters for the ring inversion process could be evaluated for six of these molecules.
V. I. P. Jones and J. A. Ladd, J. Chem. Soc. B, 1971, 567 DOI: 10.1039/J29710000567
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