The crystal structure parameters for PaBr4(isostructural with ThCl4) have been determined from quantitative X-ray powder data and refined to R 0·123. The Pa–Br bond distances are 2·77 and 3·07 Å; a value of 1·63 Å is deduced for the covalent single-bond radius of PaIV.
D. Brown, T. J. Petcher and A. J. Smith, J. Chem. Soc. A, 1971, 908 DOI: 10.1039/J19710000908
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