Bisbenzeneiron(II) hexafluorophosphate is made in excellent yield by the reaction of FeCl3, AlCl3, and benzene followed by solvolysis and treatment with aqueous ammonium hexafluorophosphate.
J. F. Helling, S. L. Rice, D. M. Braitsch and T. Mayer, J. Chem. Soc. D, 1971, 930a DOI: 10.1039/C2971000930A
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