An-X-ray determination of the crystal structure of methanetetraylbis(triphenylphosphorane)(hexaphenylcrabodiphosphorane) shows that the angle at the central carbon atom is not 180°, 145° and 131° in the two independent molecules in the unit cell.
A. T. Vincent and P. J. Wheatley, J. Chem. Soc. D, 1971, 582a DOI: 10.1039/C2971000582A
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