The novel compound trifluoromethyl hydroperoxide, CF3OOH, can be conveniently prepared by decomposition of the “perhydrate” of hexafluoroacetone, HOC(CF3)2OOH, which is produced by the 1:1 addition of hydrogen peroxide and hexafluoroacetone.
C. T. Ratcliffe, C. V. Hardin, L. R. Anderson and W. B. Fox, J. Chem. Soc. D, 1971, 784 DOI: 10.1039/C29710000784
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