The 2-methylfluorene recovered from the pyrolysis of the bis [phenyl(p-tolyl)methyl] oxalate is shown to arise from fragmentation to a carbene, thereby providing the first example of a carbene-producing pathway competing with the production of radicals in oxalate pyrolysis.
R. E. Lehr and J. M. Wilson, J. Chem. Soc. D, 1971, 666 DOI: 10.1039/C29710000666
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