An X-ray crystal study of NH4MoO2F3 has shown that MoO2F3–1 anions exist in infinite chains formed by fluorine bridging atoms; in each MoO2F4 octahedron two terminal oxygen atoms are cis-related and the bridging fluorine atoms are trans to the oxygen atoms.
L. O. Atovmyan, O. N. Krasochka and M. Ya. Rahlin, J. Chem. Soc. D, 1971, 610 DOI: 10.1039/C29710000610
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