Simple micro methods are described for the determination of nitrate based on its reduction with iodide or iodine in the presence of halogen acids. Nitric oxide gas is liberated and iodine(I) is the oxidation product from both iodide and iodine.
S. S. M. Hassan, Analyst, 1971, 96, 59 DOI: 10.1039/AN9719600059
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