The condensed-phase heats of formation of the 1:1 and 1:2 complexes of titanium tetrachloride with phosphoryl chloride have been determined by use of a reaction calorimeter as 73·5 and 87·0 kJ mol–1 respectively. Vapour pressure measurements on the complexes showed them to be completely dissociated in the gas phase.
B. Hessett and P. G. Perkins, J. Chem. Soc. A, 1970, 3331 DOI: 10.1039/J19700003331
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