A detailed analysis of the limiting low temperature 1H n.m.r. spectrum of tricarbonylcyclo-octatetraeneosmium as an eight-spin system is described, and the nature of the intramolecular process, which results in the observation of only a single line 1H n.m.r. spectrum at room temperature, is discussed.
M. Cooke, R. J. Goodfellow, M. Green, J. P. Maher and J. R. Yandle, J. Chem. Soc. D, 1970, 565b DOI: 10.1039/C2970000565B
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