It is demonstrated that the newly available αβ-acetylenic ketoximes undergo Beckmann rearrangements and/or fragmentations with PCl5 in ether, and, contrary to previous report, the products of the reaction are readily isolated and characterised.
Z. Hamlet and M. Rampersad, J. Chem. Soc. D, 1970, 1230 DOI: 10.1039/C29700001230
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