The equilibration of diastereomeric rotational isomers of 4,6-diamino-1,2-dihydro-2-methyl-1-(o-tolyl)-s-triazine hydrochloride (I), and 5-methyl-3-α-naphthyl-2-thiohydantoin (II) has been followed by integration of their n.m.r. spectra, and the activation parameters for hindered rotation about C–N bonds have been calculated.
W. E. Bentz, L. D. Colebrook, J. R. Fehlner and A. Rosowsky, J. Chem. Soc. D, 1970, 974 DOI: 10.1039/C29700000974
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