4-Amino-5-aminomethyl-1,2,3-triazoles, further substituted in the 1-, 2-, or 3-position by a methyl- or benzyl-group, were made by reducing the corresponding 4-amino-5-cyanotriazoles, obtained by the reaction of 4-amino-1,2,3-triazole-5-carboxamides with phosphoryl chloride in dimethylformamide [4-dimethylaminomethyleneamino-analogues, e.g.(III), were isolated as intermediates].
A. Albert, J. Chem. Soc. D, 1970, 858 DOI: 10.1039/C29700000858
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