The sequence: oxiran (VI)→ hydroxy-azide (VII)→ hydroxy-amine (III)→ ketone, using novel reaction conditions, provides a convenient general route for the preparation of D-homo-steroids.
D. N. Kirk and M. A. Wilson, J. Chem. Soc. D, 1970, 64b DOI: 10.1039/C2970000064B
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