The spin-coupling constants in di-t-butyl-fluorophosphine and their signs relative to 1JCH > 0 have been investigated by a heteronuclear INDOR-technique showing that 1JPF < 0 and 1JPC < 0.
C. Schumann, H. Dreeskamp and O. Stelzer, J. Chem. Soc. D, 1970, 619 DOI: 10.1039/C29700000619
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