Reversible i.r. and 1H n.m.r. spectral changes in the temperature range 28 to –45° are reported for the complex [Mo-(π-C5H5)(CO)2N:CBu2t], and interpreted in terms of conformational changes about the multiple metal–nitrogen bond.
M. Kilner and C. Midcalf, J. Chem. Soc. D, 1970, 552 DOI: 10.1039/C29700000552
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