Methods for halogen replacement by thiol groups in di-2-chloropropyl sulphide have been examined. Hydrogenation of the corresponding Bunte salt in aqueous solution gave excellent yields of dithiols but under conditions of acidic decomposition significant amounts of isomeric dimethyl1,4,5-trithiacycloheptanes were also formed.
R. T. Wragg, J. Chem. Soc. C, 1969, 2582 DOI: 10.1039/J39690002582
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