Bis(pentafluorobenzoyl) peroxide has been prepared by treatment of pentafluorobenzoyl chloride with alkaline hydrogen peroxide. It reacted with hexafluorobenzene, pentafluorobenzene, and benzene to give low yields of fluorinated biphenyls and, in each case, pentafluorophenyl pentafluorobenzoate, also in low yield.
J. Burdon, J. G. Campbell and J. C. Tatlow, J. Chem. Soc. C, 1969, 822 DOI: 10.1039/J39690000822
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