A total synthesis of magnoline (I) has been achieved by the Ullmann reaction between (+)-L-7-benzyloxy-1-(4-benzyloxy-3-bromobenzyl)-6-methoxy-2-methyl- and (–)-D-7-benzyloxy-1-(4-hydroxybenzyl)-6-methoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline. Spectroscopic comparisons between magnoline and its antipode or diastereoisomer are also described.
T. Kametani, H. Iida and K. Sakurai, J. Chem. Soc. C, 1969, 500 DOI: 10.1039/J39690000500
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