µ-Oxido-bis[triphenylphosphinenitrosyliridium(I)]–C6H6 has been prepared by the reaction of trans-Ir(CO)Cl(PPh3)2 and nitrite ion in benzene–aqueous alcohol: its structure contains the first example of a bent iridium–iridium bond and a nitrosyl group π-bonded to an iridium atom.
P. Carty, A. Walker, M. Mathew and G. J. Palenik, J. Chem. Soc. D, 1969, 1374b DOI: 10.1039/C2969001374B
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